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Fermentation quality, rumen degradability and methane emissions of mixed silages from oil palm fronds and Jack bean plants

Muhammad Ridla1,2, Nahrowi1,2, Luki Abdullah1,2 and Sudradjat3

1 Department of Animal Nutrition and Feed Technology, Faculty of Animal Science, IPB University, Kampus Dramaga, Bogor 16680, Indonesia
hmridla@apps.ipb.ac.id
2 Center for Tropical Animal Studies (CENTRAS), IPB University, Kampus IPB Baranangsiang, Jl. Raya Pajajaran, Bogor 16153, Indonesia
3 Department of Agronomy and Horticulture, Faculty of Agriculture, IPB University, Kampus Dramaga, Bogor 16680, Indonesia

Abstract

This study evaluated the effects of incorporating Jack bean plants (Canavalia ensiformis) into oil palm frond silage on nutrient composition, fermentation quality, rumen degradability and methane emissions using an in vitro system. Silage mixtures were formulated with 0%, 25%, and 50% Jack bean inclusion. Increasing Jack bean levels significantly (p< 0.05) enhanced crude protein content (9.55% to 12.32% DM) while reducing fiber fractions, including NDF, ADF, and lignin, indicating improved silage digestibility. All silages were well preserved, as shown by low dry matter (DM) loss (1.28–1.83%), low pH (4.02–4.42), low ammonia nitrogen (0.06–0.14% DM), and high Flieg point scores (119.48–129.50). Higher Jack bean inclusion increased (p<0.05) total short-chain fatty acids and rumen ammonia, leading to significantly greater dry matter and organic matter degradability. Conversely, methane production decreased sharply (p<0.05), from 4.58% to 1.67% of the total gas. These findings demonstrate that Jack bean inclusion improves silage quality, enhances nutrient utilization, and reduces environmental impact by lowering methane emissions. Optimal performance was achieved with a 50% Jack bean inclusion, which balances protein enrichment and methane mitigation.

Keywords: antinutritional factors, greenhouse gas mitigation, silage quality, sustainable feeding strategies, tropical forage


Introduction

Forages are a vital component of ruminant diets, providing essential nutrients for maintenance, growth and production (Ridla and Nahrowi 20025). However, in tropical regions like Indonesia, the consistent availability of high-quality forage is often constrained by seasonal fluctuations, leading to feed shortages, particularly during the dry season (Kumalasari et al 2025). One potential solution is the utilization of agricultural by-products as an alternative forage source (Ridla et al 2025a). Oil palm fronds, generated through routine pruning, are produced in large quantities due to Indonesia’s extensive oil palm industry (Ridla et al 2023a). In 2024, national oil palm production reached 47,474 tons, producing approximately 10.4 million tons of frond waste annually (BPS 2024). This biomass represents a sustainable and low-cost resource for ruminant feeding.

Despite its abundance, oil palm fronds have low nutritional value, such as low crude protein (CP) and high levels of structural carbohydrates, such as neutral detergent fiber (NDF) and acid detergent fiber (ADF), which limit digestibility and rumen microbial activity (Ridla et al 2023a). Combining oil palm fronds with high-protein forages is essential to enhance their feeding value. Jack bean plants (Canavalia ensiformis) are a promising option due to their high biomass yield and crude protein content ranging from 17.32% to 19.91% at 55 to 90 days after planting (Bayu et al 2025). However, Jack bean plants contain hydrogen cyanide (HCN), an antinutritional factor that can be toxic if not properly managed (Alifianty et al 2023).

Silage production is an effective method to preserve forage while reducing antinutritional compounds through microbial fermentation (Wang et al 2022). Proper silage fermentation requires sufficient water-soluble carbohydrates (WSC) as a substrate for lactic acid bacteria (LAB). Since oil palm fronds are low in WSC, adding external carbohydrate sources, such as cassava pulp and tofu waste, can enhance fermentation quality and silage stability (Ridla and Nahrowi 2025; Ridla et al 2023a).

Beyond improving feed quality, ruminant nutrition strategies must also consider environmental sustainability, particularly methane (CH₄) emissions from enteric fermentation, a significant source of greenhouse gases (Ridla et al 2023b; Ridla and Nahrowi 2025). High-fiber, low-digestibility forages typically increase CH₄ production, making it crucial to evaluate how mixed silages impact rumen fermentation and methane emissions (Ridla et al 2023b; Ridla et al 2025b).

To date, limited research has explored the combined use of oil palm fronds and Jack bean plants in silage production. Therefore, this study aimed to evaluate silage quality, in vitro rumen degradability, and methane emissions of mixed silages formulated from oil palm fronds and Jack bean plants, supporting the development of sustainable feeding strategies using underutilized agricultural by-products.


Materials and methods

Silage preparation

Oil palm fronds and Jack bean plants were used as the primary materials for silage production. Both forage materials were cultivated at the experimental plantation of IPB University, located in Jonggol, Bogor, Indonesia. The oil palm fronds were collected as a by-product of routine pruning, while the Jack bean plants were harvested at the vegetative stage to ensure optimal nutrient content (90 days after planting). The materials were chopped into 1-2 cm pieces using a mechanical chopper and mixed at predetermined ratios.

The silage was prepared by mixing oil palm fronds and Jack bean plants at different ratios. Glucose (spoiled sugar) was added at 5% of dry weight as an external water-soluble carbohydrate (WSC) source to support lactic acid bacteria (LAB) fermentation. Approximately 500 g of each mixture was tightly packed into anaerobic silos (polyethylene bottles), ensuring minimal air pockets, and sealed to prevent oxygen penetration. The silos were stored at room temperature (27-30 °C) for 40 days to allow fermentation.

Experimental design

The experiment followed a completely randomized design (CRD) with three treatments and five replicates per treatment:

T1. Oil palm fronds silage only (control).

T2. Mixed silage of oil palm fronds and Jack bean plants (75:25 fresh basis).

T3. Mixed silage of oil palm fronds and Jack bean plants (50:50 fresh basis).

After 40 days, the silages were opened for analysis of fermentation characteristics, chemical composition. In addition, in vitro rumen fermentation, gas production, methane emission, and dry and organic matter degradability were also evaluated

Chemical composition analysis

Samples were dried at 60 °C for 48 h and ground through a 1-mm screen for subsequent analyses. The following parameters were determined: dry matter (DM), crude protein (CP), ether extract (EE), crude fiber (CF), and crude ash using AOAC (2015) official methods. Neutral detergent fiber (NDF) and acid detergent fiber (ADF) were analyzed following AOAC (1990). Hemicellulose was calculated as NDF-ADF. Water-soluble carbohydrate (WSC) content was measured using the anthrone-sulfuric acid method (Deriaz 1961). Hydrogen cyanide (HCN) levels were determined using the Volhard argentometric method (AOAC 2015).

Silage fermentation quality assessment

The pH of the silage was measured using a digital pH meter (Horiba-18) after extracting 40 g of silage with 400 mL of distilled water, followed by filtration of the extract. Ammonia nitrogen (NH₃-N) concentration was determined according to AOAC (2015). The Flieg score, used to evaluate overall silage quality, was calculated using the formula = 220 + (2 × % dry matter of silage − 15) − 40 × pH as described by Kilic (1986).

In vitro rumen fermentation and degradability

Rumen fluid was collected from two rumen-fistulated cattle maintained on a standard diet containing 60% forage and 40% concentrate. The collected fluid was filtered through four layers of cheesecloth while continuously flushed with CO₂ to maintain anaerobic conditions.

The in vitro incubation was performed using the two-stage technique of Tilley and Terry (1963). Approximately 500 mg of silage sample was incubated with 50 mL of buffered rumen fluid in sealed serum bottles at 39 °C. After incubation, the residues were filtered, dried,ashed and weighed to determine in vitro dry matter degradability (IVDMD) and in vitro organic matter degradability (IVOMD).

Additionally, after 4 h of incubation, aliquots were analyzed for pH using a digital pH meter (Horiba-18), ammonia nitrogen (N-NH₃) using the Conway and O’Malley (1942) micro-diffusion method, and total short-chain fatty acids (TSCFA) via steam distillation following Kromann et al (1967).

Gas production was measured at 3, 6, 12, 24, and 48 h using a gas-tight syringe. At 48 h, the total gas volume was recorded, and a 5 mL gas sample was collected for methane (CH₄) analysis using gas chromatography, following the protocol of Theodorou et al (1994).

Statistical analysis

All data were analyzed using one-way ANOVA in SPSS version 25.0 (IBM Corp 2017). The differences among treatment means were analyzed using Tukey's Honestly Significant Difference (HSD) test to determine pairwise comparisons at a significance level of p < 0.05. Results are presented as mean ± standard deviation (SD).


Results and discussion

Chemical composition of oil palm fronds and Jack bean plants

The chemical composition of oil palm fronds and Jack bean plants is shown in Table 1. Oil palm fronds exhibited higher fiber fractions, including NDF (66.57%), ADF (27.85%), and hemicellulose (38.71%), indicating low digestibility and limited energy availability. In contrast, Jack bean plants contained higher crude protein (15.56%) and lower fiber content (NDF 40.33%), making them a valuable protein source for ruminant diets. However, the presence of hydrogen cyanide (HCN) at 303.24 ppm in Jack bean plants poses a potential toxicity risk if not adequately processed or mixed with other forages. Therefore, ensiling oil palm fronds with Jack bean plants can help balance protein and energy levels while enhancing overall feed quality and safety.

Table 1. The chemical composition of oil palm fronds and Jack bean plants

Parameter

Oil palm fronds

Jack bean plants

Dry matter (DM), %

33.07

30.15

Ash, % DM

10.00

8.31

Crude protein, % DM

8.72

15.56

Ether extract, % DM

4.50

4.02

Crude fiber, % DM

35.64

31.28

Nitrogen-free extract, % DM

41.14

40.83

Neutral detergent fiber, % DM

66.57

40.33

Acid detergent fiber, % DM

27.85

26.72

Hemicellulose, % DM

38.71

13.62

Cellulose, % DM

19.36

18.45

Lignin, % DM

7.47

7.40

Water-soluble carbohydrates, % DM

1.39

1.24

Hydrogen cyanide, ppm

-

303.24

Silage chemical composition

The inclusion of Jack bean plants in silage mixtures significantly (p<0.05) influenced nutrient composition (Table 2). Increasing Jack bean levels from 0% to 50% resulted in a progressive rise in crude protein content, from 9.55% to 12.32% DM, demonstrating its value as a protein-rich forage. In contrast, crude fiber, NDF, ADF, cellulose, and lignin concentrations decreased (p<0.05) with higher Jack bean inclusion, indicating improved degradability and potentially greater nutrient availability for ruminants. Water-soluble carbohydrates (WSC) ranged from 4.10% to 4.47% DM, providing sufficient substrate to support lactic acid bacteria activity during fermentation, which enhances silage preservation and quality. However, hydrogen cyanide (HCN) was detected at 90.94 ppm in the 25% inclusion level and increased to 140.84 ppm at 50%, posing potential toxicity risks if not carefully managed. Overall, Jack bean inclusion improves nutrient balance and silage quality, but proper control of HCN levels is essential for safe utilization.

Table 2. The chemical composition of mixed silages

Parameter

Jack bean plants' inclusion

Values

Dry matter (DM), %

0

36.21 ± 3.00

25

35.44 ± 0.79

50

37.56 ± 1.09

Ash, % DM

0

10.78 ± 1.19b

25

9.66 ± 0.84a

50

9.48 ± 0.55a

Crude protein, % DM

0

8.55 ± 0.83b

25

11.28 ± 0.16b

50

12.82 ± 0.25c

Ether extract, % DM

0

4.15 ± 0.86

25

4.39 ± 0.65

50

4.92 ± 1.08

Crude fiber, % DM

0

30.85 ± 1.07c

25

29.56 ± 1.50b

50

27.46 ± 1.68a

Nitrogen-free extract, % DM

0

44.68 ± 1.69

25

45.11 ± 1.57

50

45.83 ± 0.94

Neutral detergent fiber, % DM

0

72.25 ± 2.83b

25

68.60 ± 1.68a

50

68.13 ± 1.64a

Acid detergent fiber, % DM

0

43.74 ± 3.13b

25

41.77 ± 2.17a

50

41.03 ± 2.30a

Hemicellulose, % DM

0

28.51 ± 2.41

25

26.83 ± 1.84

50

27.10 ± 2.14

Cellulose, % DM

0

34.11 ± 2.87b

25

3 3.09 ± 2.49ab

50

32.48 ± 2.45a

Lignin, % DM

0

9.06 ± 0.76b

25

8.24 ± 0.64a

50

7.98 ± 0.47a

Water-soluble carbohydrates, % DM

0

4.10 ± 0.21

25

4.31 ± 0.08

50

4.47 ± 0.11

Hydrogen cyanide, ppm

0

-

25

90.94 ± 3.32a

50

140.84 ± 15.01b

abcMeans that in the same column, without a common letter, are significant at p<0.05

Silage fermentation quality

The fermentation characteristics of the silages are presented in Table 3. The dry matter (DM) content ranged from 35.44% to 37.56%, which is within the optimal range for desirable fermentation (Ridla et al 2024; McDonald et al 1991). All silages were well preserved, as indicated by their low DM loss, low pH values, low ammonia nitrogen (NH₃-N) concentrations and high Flieg scores (Ridla et al 2025a, Ridla and Nahrowi 2025).

The DM loss ranged from 1.28% to 1.83%, suggesting efficient nutrient conservation during the ensiling process (Ridla et al 2025b). Silage pH values between 4.42 and 4.02 are considered ideal for stable lactic acid fermentation. Similarly, NH₃-N levels were low (0.06% to 0.14% of DM), indicating minimal proteolysis and effective preservation of true protein. The high Flieg score values, 119.48 to 129.50, further confirmed the superior fermentation quality (Ridla et al 2025a; Ridla and Uchida 1998).

Overall, these findings demonstrate that all silages underwent proper fermentation and were effectively stabilized during storage, ensuring both high feed quality and nutrient retention (Muck et al 2018; Kung et al 2018).

Table 3. Silage fermentation quality

Parameter

Jack bean plants' inclusion

Values

Dry matter loss, %

0

1.83 ± 0.30b

25

1.28 ± 0.61a

50

1.78 ± 0.56b

pH

0

4.42 ± 0.06c

25

4.09 ± 0.12b

50

4.02 ± 0.04a

Flieg score

0

120.50 ± 5.56a

25

129.50 ± 4.36b

50

119.48 ± 2.88a

N-NH3,% Total N

0

0.14 ± 0.04

25

0.10 ± 0.04

50

0.06 ± 0.02

abcMeans that in the same column, without a common letter, are significant at p<0.05

Rumen fermentation, gas production, and methane emission

The inclusion of Jack bean plants in silage mixtures had a significant (p<0.05) effect on rumen fermentation, degradability, and methane production (Table 4). Rumen pH remained stable across treatments (7.13-7.09), indicating a balanced fermentation environment suitable for microbial activity. Rumen ammonia (NH₃) concentration increased significantly with higher Jack bean inclusion, from 5.79 mM (0%) to 8.98 mM (50%), reflecting greater protein availability from the Jack bean plants (Ridla et al 2025a). Total short-chain fatty acids (SCFA), key indicators of fermentation efficiency, also increased markedly, from 71.78 mM in the control to 137.88 mM at 50% inclusion, suggesting enhanced microbial fermentation (Ridla et al 2025b).

Degradability parameters improved significantly (p<0.05) with the inclusion of Jack bean plants. Dry matter degradability increased from 52.33% at 0% to 64.40% at 50%, while organic matter degradability showed a similar improvement, rising from 51.31% to 63.06%. These results indicate enhanced nutrient utilization due to the higher proportion of digestible forage contributed by Jack bean plants (Ridla et al 2023a). Total gas production also increased significantly, reflecting greater microbial fermentation activity with higher Jack bean inclusion (Ridla and Nahrowi 2025).

Table 4. Rumen fermentation, digestibility, and methane production

Parameter

Jack bean plants' inclusion

Values

Rumen pH

0

7.13 ± 0.04

25

7.11 ± 0.04

50

7.09 ± 0.05

Rumen ammonia, mM

0

5.79 ± 1.27a

25

7.35 ± 1.02b

50

8.98 ± 0.67c

Total short-chain fatty acid, mM

0

71.78 ± 12.22a

25

107.81 ± 10.41b

50

137.88 ± 10.03c

Dry matter degradability, %

0

52.33 ± 2.56a

25

56.22 ± 1.95b

50

64.40 ± 2.35c

Organic matter degradability, %

0

51.31 ± 2.62a

25

55.12 ± 1.52b

50

63.06 ± 2.05c

Total gas production, ml/g Dry matter

0

58.56 ± 5.86a

25

71.24 ± 5.26b

50

101.53 ± 9.36c

CH4, % Total gass

0

4.58 ± 0.68a

25

2.91 ± 0.56b

50

1.67 ± 1.08c

CH4, % Organic matter digestibility

0

1.41 ± 0.27a

25

0.64 ± 0.15b

50

0.31 ± 0.21a

abcMeans that in the same column, without a common letter, are significant at p<0.05

Interestingly, methane (CH₄) production decreased sharply with increasing Jack bean plant inclusion. CH₄ as a percentage of total gas dropped from 4.58% in the control to 1.67% at 50% inclusion. Similarly, CH₄ production per unit of organic matter digestibility declined, indicating improved fermentation efficiency and reduced energy loss through methane emissions. Overall, incorporating Jack bean plants, a more digestible and nutrient-rich forage, into silage mixtures enhanced rumen fermentation, improved degradability, and promoted environmental sustainability by mitigating methane production (Ridla et al 2023a; Ridla and Nahrowi 2025).


Conclusion


Acknowledgements

The authors gratefully acknowledge the financial support provided by IPB University through the Skema Riset Aksi, under grant number 15328/IT3.D10/PT.01.03/P/B/2024. This funding was essential for the successful implementation and completion of this research project.


References

Alifianty O F, Ridla M, Nahrowi, Martin R S H and Akhadiarto S 2023 Optimization of Jack bean ( Canavalia ensiformis L.) processing to reduce hydrogen cyanide content and enhance broiler chicken performance: a potential alternative to soybeans in poultry feed. Livestock Research for Rural Development. Volume 35, Article #68. http://www.lrrd.org/lrrd35/8/3568hmri.html

AOAC 1990 Fiber (acid detergent) and lignin in animal feed (method 973.18). In: Association of Official Analytical Chemists. 15th edition. Washington, DC (US).

AOAC 2015 Official Methods of Analysis. Association of Official Analytical Chemists. 18th eds. Arlington (US).

Bayu P, Bambang S, Genki I, Takahiro G, Diafan K J and Yogi SP 2025 Nutrient content of Jack bean (Canavalia ensiformis) at different growth stages in Blora, East Java, Indonesia. BIO Web of Conferences. 164, 02001. https://doi.org/10.1051/bioconf/202516402001

BPS 2024 Badan pusat statistika. Produksi tanaman perkebunan. Retrieved September 20, 2025. https://www.bps.go.id/id/statistics-table/2/MTMyIzI=/produksi-tanaman-perkebunan.html

Conway E J and O’Malley E 1942. Microdiffusion methods. Ammonia and urea using buffered absorbents (revised methods for ranges greater than 10 μg N). Biochemical Journal. 36, 655–661, https://doi.org/10.1042/bj0360655

Deriaz R E 1961 Routine analysis of carbohydrates and lignin in herbage. Journal of the Science of Food and Agriculture. 12, 150–160, https://doi.org/10.1002/jsfa.2740120210

IBM Corp 2017 IBM SPSS Statistics for Windows, Version 25.0. IBM Corp., Armonk, NY (US)

Kilic A 1986 Silo feed (instruction, education, and application proposals). Bilgehan Press, 327 p.

Kromann R P, Meyer J H and Stielau W J 1967 Steam distillation of volatile fatty acids in rumen ingesta. Journal of Dairy Science. 50, 73–76, https://doi.org/10.3168/jds.S0022-0302(67)87356-9

Kumalasari N R, Suharti S, Zahra W A, Rosmalia A, Permana I G and Sunardi S 2025 Seasonal adaptation in feed management: assessing forage and feedstuff variations in small-sized dairy farms in Boyolali, Central Java. Jurnal Sain Peternakan Indonesia, 20(2), 111–116. https://doi.org/10.31186/jspi.id.20.2.111-116

Kung L, Shaver R D, Grant R J and Schmidt R J 2018 Silage review: Interpretation of chemical, microbial, and organoleptic components of silages. Journal of Dairy Science, 101(5), 4020-4033. https://doi.org/10.3168/jds.2017-13909

McDonald P, Henderson A R and Heron S J E 1991 The Biochemistry of Silage. Second Edition. By Marlow, Bucks, UK: Chalcombe Publications.

Muck R E, Nadeau E M G, McAllister T A, Contreras-Govea F E, Santos MC and Kung L Jr 2018 Silage review: Recent advances and future uses of silage additives. Journal of Dairy Science. 101, 3980–4000, https://doi.org/10.3168/jds.2017-13839

Ridla M and Uchida S 1998 Effects of combined treatment of lactic acid bacteria and cell wall degrading enzymes on fermentation and composition of Rhodes grass (Chloris gayana Kunth.) silage. Asian Australas. Journal of Animal Science. 11, 522–529, https://doi.org/10.5713/ajas.1998.522

Ridla M, Mulyanto, Setiana M A and Nahrowi 2023a Nutrient content and digestibility of silage made from mixed oil palm fronds and tofu waste. Livestock Research for Rural Development. Volume 35, Article #53. http://www.lrrd.org/lrrd35/6/3553hmri.htm

Ridla M, Asikin N, Jayanegara A and Samsudin A A 2023b Mitigating methane emissions for rural tropical livestock through selecting appropriate grass types. Livestock Research for Rural Development. Volume 35, Article #60. http://www.lrrd.org/lrrd35/7/3560hmri.html

Ridla M, Albarki H, Risyahadi S and Sukarman 2024 Effects of wilting on silage quality: a meta-analysis. Animal Bioscience. 37(7), 1185-1195. https://doi.org/10.5713/ab.23.0403

Ridla M, Jayanegara A and Nahrowi 2025a Evaluation of silage quality, rumen fermentation dynamics, degradability, and methane emissions of total mixed rations formulated from agricultural by-products: an in vitro analysis. Journal of Animal and Feed Sciences, 34(3), 442-450. https://doi.org/10.22358/jafs/200863/2025

Ridla M, Abdullah L and Ernawati A 2025b Influence of carbohydrate fractions on degradability, rumen fermentation, and methane emission in selected tropical forages using an in vitro study. Agriculture and Natural Resources. 59(3), Article 590304. https://doi.org/10.34044/j.anres.2025.59.3.04

Ridla M and Nahrowi 2025 Methane mitigation strategies by optimizing nutrient profiles in an eco-friendly mixture of cassava pulp and Indigofera zollingeriana branch silage with strategic protein supplementation. Advances in Animal and Veterinary Sciences. 13(1): 198-208. https://dx.doi.org/10.17582/journal.aavs/2025/13.1.198.208

Theodorou M K, Williams B A, Dhanoa M S, McAllan A B and France J 1994 A simple gas production method using a pressure transducer to determine the fermentation kinetics of ruminant feeds. Animal Feed Science and Technology. 48, 185–197, https://doi.org/10.1016/0377-8401(94)90171

Tilley J M A and Terry R A 1963A Two-stage technique for the in vitro digestion of forage crops. Grass and Forage Science, 18, 104-111. https://doi.org/10.1111/j.1365-2494.1963.tb00335.x

Wang N, Xiong Y, Wang X, Guo L, Lin Y, Ni K, and Yang F 2022 Effects of Lactobacillus plantarum on Fermentation Quality and Anti-Nutritional Factors of Paper Mulberry Silage. Fermentation, 8(4), 144. https://doi.org/10.3390/fermentation8040144